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02-13

Study on the new synthesis process of monochloroacetone

The gasified acetone is mixed with chlorine in a certain proportion and enters the tubular reactor to react to produce monochloroacetone. The main factors affecting the reaction such as the reaction phase, the size of the reactor and the ratio of reactants are investigated, and the appropriate reaction conditions are proposed , The product purity can reach more than 96%.
Study on the new synthesis process of monochloroacetone
02-13

The experimental part of chloroacetone

After preheating and vaporizing, monochloroacetone is sent to the tubular reactor in a certain proportion with chlorine for reaction. The reaction product is quickly condensed with chilled water and cooled to stop the deep chlorination of acetone. Collect the reaction liquid and distill to recover unreacted acetone Collect the fractions from 118 to 119.C, and analyze the purity of the product by gas chromatography. The by-product Hcl of the reaction is absorbed by water spray, and the by-product hydrochloric acid.
The experimental part of chloroacetone
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